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LITTLE IGLOOS
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STB extraction of MHRB.

Pulled with naptha.

Freeze precipitated.

Condensed the naptha that remained in the vessel on magnetic stirring hotplate.

The warm condensed product was then freeze precipitated a second time. The resulting yield was combined to the first.

Re-x using clean warm naptha.

Added a splash of anhydrous acetone to the resulting mixture to encourage a bit more rapid evaporation.

Freeze precipitation for a third time and here are the neat little crystal forms due to the acetone presence in the environment.

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7 months ago